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SEM micrographs of BaCrO4 structures. 50 mol L-1 NaOH. Reproduced with permission from Mater. Res. , 2009, 44, 288. Copyright 2009 Elsevier. Fig. 19. (a)-(c) SEM micrographs of BaCrO4 crystals prepared in the presence of both P123 and CTAB. 80 g L-1, 12 h. (d) SEM micrograph of BaCrO4 crystals prepared in the presence of CTAB. The insets of (a), (b), and (c) show the individual BaCrO4 crystal. Reproduced with permission from Mater. Res. , 2009, 44, 288. Copyright 2009 Elsevier. 20 mol L-1, the flakes consisted of particles were observed (Fig.

Microwave synthesis of SrCO3 one-dimensional nanostructures assembled from nanocrystals using ethylenediamine additive. Materials Letters, 62, 2512-2515. Ma, M. G. & Zhu, Y. J. (2007). A simple route to synthesis of SrCO3 with olive-like and flower-like morphologies, Journal of Nanoscience and Nanotechnology, 7, 4552-4556. Ma, M. ; Zhu, Y. ; Li, L. & Cao, S. W. (2008). Nanostructured porous hollow ellipsoidal capsules of hydroxyapatite and calcium silicate: preparation and application in drug delivery.

When the basicity of the basic additive increases, the sizes of CaCO3 structures decrease. However, there seems a tendency to form assembled complex morphology when using Na2CO3 as the CO32– source. There results shows that the source of carbonates has a significant influence on the morphology of CaCO3. When using Na2CO3 as the CO32- source and NaOH as an alkali additive by microwave heating at 180 oC for 20 min in 1,4-butanediol instead of EG, a completely different shape (polyhedral) of CaCO3 was observed.

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